(1) Introduction (2) Purification by Recrystallization (3) Converting one salt into another (4) Hydrolysis of p-Nitroacetanilide to p-Nitroaniline (5)Column chromatography
教學目標Course Objectives
本課程旨在增進學生對於化學實驗基本操作之認識、化學原理的印證及奠定學生基本操作技巧，進而培養其敏銳觀察、正確搜集實驗資料及合理判斷結果之能力。
This course introduces the basic operation and principal verification of chemistry, and to establish the foundational operation skill. Furthermore, it will cultivate ability of keen observation, corrective experience data collection, and reasonable judgment of the result.
先修科目Prerequisites
無
None
教學方式Teaching Methods
講課
Lecturing
學生課後書面報告
After class written report
評量方式Assessment
小組作業
Group homework
期末報告
Final report
出席狀況
Class attendance
課堂參與與表現
Class involvement
小組作業：50％；期末報告：30％；出席狀況：10%；課堂參與與表現：10%
參考書目Reference
1. Chemistry in the Laboratory (5th) J. M. Postma, J. L. Roberts Jr., J. L. Hollenberg
2. World of Chemistry (2nd) J. R. Blackburn, M. D. Joesten, P. B. Langford, J. C. Craig
3. Experiments in general Chemistry (6th) R.A.D.Wentworth
教學進度Course Schedule
2018/09/17 導論：上課須知、實驗室安全規定、實驗器材、如何撰寫報告
Introduction：Student Guidelines; Laboratory Safety Rules; Experimental Apparatuses; How to Prepare a Report
莊大賢(Ta-Hsien Chuang) 2018/10/01 檢查實驗器材
Check-in
莊大賢(Ta-Hsien Chuang) 2018/10/15 再結晶純化：實驗原理、實驗步驟、常用溶媒、如何選用溶媒、誘導結晶方法
Purification by recrystallization: Experiment Principle; Experimental Procedure; Common Solvents; How to Choose a Suitable Solvent; How to Induce the Crystallization
莊大賢(Ta-Hsien Chuang) 2018/10/29 離子轉換：實驗原理、實驗反應式、實驗步驟、酸鹼檢測、傾析法
Converting one salt into another：Experiment Principle; Chemical Equation; Experimental Procedure; Check pH; Decantantion
莊大賢(Ta-Hsien Chuang) 2018/11/12 利用化學變化製備純物質(I)：實驗原理、實驗反應式、實驗步驟、水流幫浦、氧化還原
Preparation of pure substances by chemical changes(I): Experiment Principle; Chemical Equation; Experimental Procedure; Water Circulating Vacuum Pump; Redox Reaction
莊大賢(Ta-Hsien Chuang) 2018/11/26 1.利用化學變化製備純物質(II)：實驗原理、實驗反應式、實驗步驟、銅離子檢驗 、鋅離子檢驗
2.水解反應：實驗原理、實驗反應式、實驗步驟、酸鹼中和、薄層色層分析
(1)Preparation of pure substances by chemical change(II) : Experiment Principle; Chemical Equation; Experimental Procedure; Check Copper ions; Check Zinc ions
(2)Hydrolysis of p-Nitroacetanilide to p-Nitroaniline：Experiment Principle; Chemical Equation; Experimental Procedure; Acid-base Neutralization; Thin Layer Chromatography (TLC)
莊大賢(Ta-Hsien Chuang) 2018/12/10 管柱層析法：實驗原理、實驗步驟、充填管柱、進樣、收集樣品、檢測
Column Chromatography: Experiment Principle; Experimental Procedure; Column Packing; Loading Sample; Collect Sample; Detect
莊大賢(Ta-Hsien Chuang) 2018/12/24 期末考試
Final exam.
莊大賢(Ta-Hsien Chuang) 2019/01/07 研討
Discussion
莊大賢(Ta-Hsien Chuang)